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Background: The rapid advancement of Artificial Intelligence (AI), intelligent automation, and digital technologies is reshaping workforce dynamics across industries. Organizations are increasingly adopting AI-enabled systems to improve operational efficiency, innovation, and decision-making capabilities. This transformation has led to the emergence of Workforce 5.0, a human-centric paradigm that emphasizes collaboration between human intelligence and artificial intelligence to create agile, resilient, and future-ready organizations. Objective: This review aims to examine existing research on Human–AI synergy in Workforce 5.0, with a particular focus on reskilling strategies, workforce transformation, and organizational agility frameworks that support intelligent enterprise development. Review Methodology: A comprehensive literature review was conducted using peer-reviewed journal articles, conference papers, industry reports, and scholarly publications published between 2018 and 2026. Relevant studies were identified through academic databases including Google Scholar, Scopus, IEEE Xplore, SpringerLink, and ScienceDirect. The selected literature was analyzed using thematic synthesis to identify recurring trends, challenges, and emerging frameworks related to Human–AI collaboration. Key Findings: The review reveals that Human–AI collaboration enhances productivity, innovation, decision-making quality, and workforce adaptability. AI-driven learning platforms, personalized reskilling programs, and intelligent workforce analytics emerged as critical enablers of organizational agility. The findings further indicate that organizations adopting collaborative intelligence models achieve greater resilience and competitive advantage compared to those relying solely on automation-focused approaches. Conclusion: Workforce 5.0 represents a significant shift toward human-centered digital transformation, where AI augments rather than replaces human capabilities. Successful implementation requires continuous reskilling, adaptive organizational strategies, and integrated Human–AI collaboration frameworks. The review highlights the growing importance of balancing technological advancement with workforce development to achieve sustainable organizational performance in intelligent enterprises.